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Beilstein J. Org. Chem. 2016, 12, 1839–1850, doi:10.3762/bjoc.12.173
Graphical Abstract
Figure 1: Structures of sesquiterpenes obtained by incubation of FPP with bacterial sesquiterpene cyclases.
Figure 2: Contiguous spin systems observed by 1H,1H-COSY (bold), key HMBC and NOE correlations for a) α-amorp...
Figure 3: Contiguous spin systems observed by 1H,1H-COSY (bold), key HMBC and NOE correlations for a) 7-epi-α...
Scheme 1: Biosynthetic pathway from FPP to 7-epi-α-eudesmol (4).
Figure 4: Incubation experiments with (6-13C)FPP and the 7-epi-α-eudesmol synthase in deuterium oxide. a) 13C...
Figure 5: Incubation experiments with (13-13C)FPP. 13C NMR spectra of a) unlabelled 1 and (13-13C)-1, b) unla...